| DOI: | 10.2172/1018309
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| 报告号: | SRNL-STI-2010-00755
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| 报告题名: | Qualification of a Carbon Analyzer to Support the Defense Waste Processing Facility |
| 作者: | Hansen, D.J.; Anderson, D.C.; Hall, D.B.; Greger, P.D.; Ostler, W.K.
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| 出版年: | 2011
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| 发表日期: | 2011-07-05
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| 国家: | 美国
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| 语种: | 英语
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| 中文主题词: | 碳
; 无机碳
; 有机碳
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| 主题词: | CARBON
; INORGANIC CARBON
; ORGANIC CARBON
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| 英文摘要: | The I-O Model 1030 carbon analyzer has been qualified for use at the Defense Waste Processing Facility (DWPF). The qualification was a side-by-side comparison of the Model 1030 system with the currently used Model 1010 Analyzer. This recommendation is based on side-by-side comparisons of the new unit to the currently used Model 1010 analyzer that are presented in this report. The side-by-side testing included standards and process samples. The standards, which were used for instrument calibration verifications in the measurement of total inorganic carbon (TIC) and of total organic carbon (TOC), were traceable back to the National Institute of Standards and Technology. The process samples included TIC analyses of Sludge Receipt and Adjustment Tank samples and TOC analyses for Slurry Mix Evaporator (SME) samples. After the Model 1030 has been used for production reporting, DWPF should consider an investigation into the uncertainties associated with the TOC measurements to determine how far below the 18,916 ppm limit DWPF must control the average of the measurements for a set of SME samples to account for the uncertainties of the measurements from this new analyzer. Based upon the results presented in this report, it is recommended that the Model 1030 carbon analyzer is qualified for use. This recommendation is based on side-by-side comparisons of the new unit to the currently used Model 1010 analyzer that are presented in this report. The side-by-side testing included standards for instrument calibration verifications for TIC and TOC, and process samples. The standards were traceable back to NIST. The process samples included TIC analyses of SRAT Receipt samples and TOC analyses for SME samples. At some point in the future, after the Model 1030 has been used for production reporting, DWPF should consider an investigation into the uncertainties associated with the TOC measurements to determine how far below the 18,916 ppm limit DWPF must control the average of the measurements for a set of SME samples to account for the uncertainties of the measurements from this new analyzer. |
| URL: | http://www.osti.gov/scitech/servlets/purl/1018309
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| Citation statistics: |
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| 资源类型: | 研究报告
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| 标识符: | http://119.78.100.158/handle/2HF3EXSE/40166
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| Appears in Collections: | 过去全球变化的重建
影响、适应和脆弱性
科学计划与规划
气候变化与战略
全球变化的国际研究计划
气候减缓与适应
气候变化事实与影响
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| 1018309.pdf（88KB） | 研究报告 | -- | 开放获取 | | View
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| Recommended Citation: | |
Hansen, D.J.,Anderson, D.C.,Hall, D.B.,et al. Qualification of a Carbon Analyzer to Support the Defense Waste Processing Facility. 2011-01-01.
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