globalchange  > 过去全球变化的重建
DOI: 10.1016/j.marpolbul.2014.12.022
Scopus ID: 2-s2.0-84922266258
Selective extraction and concentration of mebendazole in seawater samples using molecularly imprinted polymer as sorbent
Author: Lian Z.; Liang Z.; Wang J.
Source Publication: Marine Pollution Bulletin
ISSN: 0025-326X
EISSN: 1879-3363
Publishing Year: 2015
Volume: 91, Issue:1
pages begin: 96
pages end: 101
Language: 英语
Keyword: Adsorption ; Mebendazole ; Molecularly imprinted polymer ; Natural seawater ; Solid-phase extraction
Scopus Keyword: Adsorption ; Crosslinking ; Ethylene ; Ethylene glycol ; High performance liquid chromatography ; Phase separation ; Polymers ; Seawater effects ; Environmental water samples ; Ethylene glycol dimethacrylate ; Mebendazole ; Molecularly Imprinted Polymer ; Molecularly imprinted solid-phase extraction ; Relative standard deviations ; Solid-phase extraction ; Solid-phase extraction sorbents ; Extraction ; acetonitrile ; ethylene glycol dimethacrylate ; mebendazole ; methacrylic acid ; molecularly imprinted polymer ; non imprinted polymer ; polymer ; sea water ; sorbent ; unclassified drug ; antinematodal agent ; mebendazole ; methacrylic acid derivative ; sea water ; water pollutant ; adsorption ; concentration (composition) ; extraction method ; liquid chromatography ; organic pollutant ; polymer ; purification ; seawater ; water pollution ; adsorption kinetics ; Article ; binding affinity ; binding site ; concentration (parameters) ; controlled study ; cross linking ; desorption ; high performance liquid chromatography ; hydrogen bond ; measurement accuracy ; molecular interaction ; molecularly imprinted solid phase extraction ; reliability ; reproducibility ; scanning electron microscopy ; Scatchard plot ; sensitivity analysis ; separation technique ; solid phase extraction ; structure analysis ; surface property ; synthesis ; water analysis ; water management ; water sampling ; adsorption ; analysis ; chemistry ; ecosystem restoration ; evaluation study ; isolation and purification ; molecular imprinting ; procedures ; solid phase extraction ; water pollutant ; Adsorption ; Antinematodal Agents ; Chromatography, High Pressure Liquid ; Environmental Restoration and Remediation ; Mebendazole ; Methacrylates ; Molecular Imprinting ; Polymers ; Seawater ; Solid Phase Extraction ; Water Pollutants, Chemical
Subject of Scopus: Agricultural and Biological Sciences: Aquatic Science ; Earth and Planetary Sciences: Oceanography ; Environmental Science: Pollution
English Abstract: A high selective pre-treatment method for the extraction and analysis of mebendazole in environmental water samples was developed based on molecularly imprinted solid-phase extraction (MISPE). The mebendazole imprinted polymers were synthesized in acetonitrile using methacrylic acid and ethylene glycol dimethacrylate as functional monomer and cross-linker respectively. The imprinted materials showed high adsorption ability for mebendazole and were applied as special solid-phase extraction sorbents for selective separation of mebendazole. An off-line MISPE procedure was developed for the purification and enrichment of mebendazole from natural seawater samples prior to high-performance liquid chromatography analysis. The recoveries of spiked seawater on the MISPE cartridges were from 83.0% to 90.6%, and the values of the relative standard deviation were in the range of 2.78-4.13% (n = 3). The satisfied results showed that this pre-treatment methodology for extracting mebendazole in seawater was simple and effective. © 2014 Elsevier Ltd.
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被引频次[WOS]:8   [查看WOS记录]     [查看WOS中相关记录]
Document Type: 期刊论文
Appears in Collections:过去全球变化的重建

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Affiliation: Marine College, Shandong University, Weihai, China; Key Laboratory of Marine Chemistry Theory and Technology, Ministry of Education, College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao, China

Recommended Citation:
Lian Z.,Liang Z.,Wang J.. Selective extraction and concentration of mebendazole in seawater samples using molecularly imprinted polymer as sorbent[J]. Marine Pollution Bulletin,2015-01-01,91(1)
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